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Catalytic activities of heterogeneous catalysts obtained by copolymerization of metal-containing 2-(acetoacetoxy)ethyl methacrylate

Among the synthetic strategies commonly used for supporting a metal complex onto an organic polymer in order to obtain an heterogenous catalyst, a valid choice is to synthesize a metal containing monomer (MCM), which can subsequently be subjected to polymerization with suitable comonome...

Cascade Fractional-Order PI Control of a Linear Positioning System

This paper proposes a method for designing robust fractional-order proportional-integral (FOPI) controllers to be employed in a cascade control system. The FOPI controllers are employed for controlling two nested loops. The design is based on performance and robustness specifications in the ...

31P and195Pt solid-state NMR and DFT studies on platinum(i) and platinum(II) complexes

31P and195Pt solid state NMR spectra of anti-[(PHCy)ClPt(μ-PCy2)2Pt(PHCy)Cl] (3) and [(PHCy2)Pt(μ-PCy2)(κ2P,O-μ-POCy2)Pt(PHCy2)] (Pt-Pt) (4) were recorded under cross polarization/magic-angle spinning conditions (31P) or with the cross polarization/Carr-Purcell-Meiboom-Gill pulse sequence (195Pt) and compared to the data...

Dinuclear and tetranuclear copper(I) iodide complexes with P and P^N donor ligands: Structural and photoluminescence studies

In order to investigate photophysical properties and crystallization medium effects, three Cu complexes, [CuI(PCy3)]2(1), [Cu(I)(PPh2Me)]4(2), and [Cu4(I)4(PPh2py)2] (3) were prepared and characterized using single crystal X-ray crystallography, solid state NMR, UV–Vis, and IR spectroscopy. In 1, as previously&...

Uncertainty Evaluation of the Unified Method for Thermo-Electric Module Characterization

In this paper the uncertainty evaluation of the recently proposed Unified Method for Thermo-Electric Module characterization is carried out. The measurement model is detailed and individual uncertainty contributions are highlighted, with close reference to the instrumentation and measurement setup. Th...

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